ASTM E1508 PDF

Find the most up-to-date version of ASTM E at Engineering Buy ASTM E GUIDE FOR QUANTITATIVE ANALYSIS BY ENERGY- DISPERSIVE SPECTROSCOPY from SAI Global. Standard Guide for Quantitative Analysis by Energy-Dispersive Spectroscopy. Status: Withdrawn ยท Replaced by: ASTM E Buy this standard. Price: SEK.

Author: Guktilar Nall
Country: South Africa
Language: English (Spanish)
Genre: Photos
Published (Last): 17 November 2015
Pages: 245
PDF File Size: 19.92 Mb
ePub File Size: 2.93 Mb
ISBN: 781-5-59034-947-9
Downloads: 54715
Price: Free* [*Free Regsitration Required]
Uploader: Nikor

Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. Elements of lower atomic number than sodium can be analyzed with either ultra-thin-window or windowless spectrometers, generally with less precision than is possible for heavier elements.

However, most matrix e1580 programs are sufficiently r1508 to permit the use of pure element standards. Evaporated carbon is usually the most suitable coating material. This method is not based on any model and, therefore, is more general.

Accordingly, before routinely using aatm standardless method for quantitative analysis, it is important to validate the method for a particular class of materials by comparing it against analysis with standards or against a completely different quantitative technique, such as X-ray?

Light Element Analysis Observing the high-energy cutoff of the continuum, as noted in 8. Requiring set parameters had little effect on the repeatability but improved the reproducibility for chromium and iron, but not for nickel. For quantitative analysis, a shaping time of about 10?

Practice E is used to analyze the round-robin data for asfm and calculates intralaboratory repeatability and interlaboratory reproducibility statistics. Specimens mounted in a nonconducting medium must make electrical contact with the microscope stage.

ASTM E – 12a Standard Guide for Quantitative Analysis by Energy-Dispersive Spectroscopy

If asstm stoichiometry of compounds containing light elements is known, then calculation by stoichiometry is wstm most accurate method. Two methods in common use are 1 the method of overlap factors and 2 the method of multiple least squares. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

  INGRESARIOS LIBRO PDF

ASTM B r The asrm cannot occur at energies below the absorption edge of the Si K line, and it becomes negligible at higher energies such as the Cu Ka line. These errors arise from the different ways various systems generate the pure element intensities, rather than from differences in ZAF or phi-rho-z matrix corrections.

Elements ee1508 lower atomic number than sodium can be analyzed with either ultra-thin-window or windowless spectrometers, generally with less precision than is possible for heavier elements. The report should also specify whether standards or standardless ashm were used, what matrix corrections were applied, and whether any elemental concentrations were calculated by difference or by stoichiometry.

It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. E1058 metals such as gold that are often used for SEM imaging are less suitable because they heavily absorb X rays; if the coating is thick enough, X-ray lines from those metals will be seen in the spectrum.

For the alloy MAthe average was 3. The actual accelerating voltage of the electron beam does not always correspond with the voltage selected on the instrument.

Both specimens were analyzed by various metal producers, EDS system manufacturers, and one university. It includes both methods that use standards as well as standardless methods, and it discusses the precision and accuracy that one Copyright?

ASTM E1508 – 12a

If asfm sample is not tilted, the take-off angle is de? If they are etched, the operator must make sure that the composition in the region to be analyzed has not been altered and that aastm region to be analyzed is? Accordingly, most operators choose a 0โ€”10 keV display at higher display resolution rather than a 0โ€”20 keV display at lower resolution. There are several expressions in use by commercial manufacturers to calculate this, and all produce similar results if the tilt angle is not extreme.

  ASKEP NEFROLITIASIS PDF

Vertical distance is the distance from the bottom of the pole piece of the?

Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility. These conditions include the accelerating voltage, take-off angle and tilt, and the analytical line KLM used. A number in parentheses indicates the f1508 of last reapproval.

ASTM E – 12 Standard Guide for Quantitative Analysis by Energy-Dispersive Spectroscopy

It was requested that analyses by both standards and standardless methods be reported. It can be determined ast, expanding the vertical scale asgm the EDS spectrum and observing the energy above which continuum X rays do not occur.

On the MA alloy, the reproducibility among laboratories was much less than that of the standards technique R in Table 4. The intensity of such X rays is proportional to the mass fraction of that element in the specimen. Last previous edition approved in as E โ€” Often aluminum and copper are used, and sometimes both the K and L lines of copper are used. This is because a correction is necessary to account for the effect of other elements the matrix present in the specimen.

If that X ray escapes from the detector, its energy that would ordinarily have been measured is lost. In like manner, deconvolution routines work well in most cases, but not when the overlapped lines arise from elements present in widely different concentrations. This requirement does not preclude scratches; however, any scratches in the immediate vicinity of the analyzed region must be insigni?

Sr SR Nickel 9. The interlaboratory reproducibility under standard conditions averaged 8.